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Employment of modern analytical methods for adsorption studies and pharmaceutical analysis
- Date Issued:
- 1997
- Summary:
- Ultraviolet spectrophotometry was employed to investigate the adsorption of phenylphosphonic acid onto the surface of alumina from aqueous solution. It was found that an initial chemisorption occurred with monolayer coverage, reaching a maximum at a solution pH of 3.0. The results were interpreted as indicating that this and related adsorptions are controlled by ligand exchange processes involving electrostatic attraction between oppositely-charged species. In a separate project, high performance liquid chromatography was employed for the quantitative analysis of aminophylline in commercial thigh cream formulations. The analysis required derivatization of the compound by dansylation under carefully-controlled conditions. This enhanced its detection and separation from other cream components.
Title: | Employment of modern analytical methods for adsorption studies and pharmaceutical analysis. |
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Name(s): |
Foss, Wendy Marie Florida Atlantic University, Degree Grantor Haky, Jerome E., Thesis Advisor |
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Type of Resource: | text | |
Genre: | Electronic Thesis Or Dissertation | |
Issuance: | monographic | |
Date Issued: | 1997 | |
Publisher: | Florida Atlantic University | |
Place of Publication: | Boca Raton, Fla. | |
Physical Form: | application/pdf | |
Extent: | 77 p. | |
Language(s): | English | |
Summary: | Ultraviolet spectrophotometry was employed to investigate the adsorption of phenylphosphonic acid onto the surface of alumina from aqueous solution. It was found that an initial chemisorption occurred with monolayer coverage, reaching a maximum at a solution pH of 3.0. The results were interpreted as indicating that this and related adsorptions are controlled by ligand exchange processes involving electrostatic attraction between oppositely-charged species. In a separate project, high performance liquid chromatography was employed for the quantitative analysis of aminophylline in commercial thigh cream formulations. The analysis required derivatization of the compound by dansylation under carefully-controlled conditions. This enhanced its detection and separation from other cream components. | |
Identifier: | 9780591333978 (isbn), 15404 (digitool), FADT15404 (IID), fau:12171 (fedora) | |
Note(s): | Thesis (M.S.)--Florida Atlantic University, 1997. | |
Subject(s): |
Adsorption Spectrophotometry Chromatographic analysis Solution (Chemistry) |
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Held by: | Florida Atlantic University Libraries | |
Persistent Link to This Record: | http://purl.flvc.org/fcla/dt/15404 | |
Sublocation: | Digital Library | |
Use and Reproduction: | Copyright © is held by the author with permission granted to Florida Atlantic University to digitize, archive and distribute this item for non-profit research and educational purposes. Any reuse of this item in excess of fair use or other copyright exemptions requires permission of the copyright holder. | |
Use and Reproduction: | http://rightsstatements.org/vocab/InC/1.0/ | |
Host Institution: | FAU | |
Is Part of Series: | Florida Atlantic University Digital Library Collections. |